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HomeMy WebLinkAboutST - 3301 S NORFOLK ST - ASSOCIATED GROCERS - STORAGE TANKSTANKS) UNDERGROUND STORAGE TANKS (UST) I ABOVE GROUND STORAGE TANKS (AST) 3301 S NORFOLK ST RELATED PERMIT NUMBER(S) 6-19 7-19 360-92 3301 S NORFOLK 2/ h UNDERGROUND STORAGE TANK / Date: 6/26/92 TUKWILA FIRE DEPARTMENT SPECIAL PERMIT No. 360-92 BY virtue of The Provisions of the Uniform Fire Code adopted by City of Tukwila Ordinance, Global Diving & Salvage, Inc. located at 3301 South Norfolk Business Name Business Address having made application in due form, and as the conditions, surroundings, and arrangements are, in my opinion, such that the intent of the Ordinance can be observed, authority is hereby given and this PERMIT is granted for*TO install, alter, remove, place temporarily out of service or otherwise dispose of any flammable or combustible liquid_tank_per 79..104 of rhe____ Uniform Fire Code* This PERMIT is issued and accepted on condition that all Ordinance provisions now adopted, or that may hereafter be adopted, shall be complied with. THIS PERMIT VALID FOR -June 26, 1992 thru July 26, 1992 - This permit does not take the place of any license required by law and is not transfer- able. ransferable. Any change in the use or occupancy of premises shall require a new permit. Fire Marshal THIS PERMIT MUST BE POSTED ON THE PREMISES MENTIONED ABOVE 16. T.F.D./F.P. #2 TUKWILA FIRE DEPARTMENT UNDERGROUND FUEL TANK REMOVAL/INSTALLATION PERMIT PERMIT # 3lla -'2 RECEIPT # 7395- DATE RECEIVED (!--(C.12-- DATE ISSUED CODE REFERENCE: 79.114 FIRM NAME: PHONE : ZCxo' . M2-- I FIRM ADDRESS: JOB SITE: A 9 &t Pcra 7 cAs2.05 /3"at S ' No12FoLK./6vAc Ti. ,v43. .'1&' NUMBER OF TANKS TO BE REMOVED/ STA LED: (1) Ot'4 Fi 4c-4 - 77t1: L NAME OF BUSINESS AT JOB SITE: 5044AlE:. tj,/E PERSON IN CHARGE: C7541_ PHONE: 2CZ'o.((o2 •p1 PAS'( G 7 ' t- 7r CLc�t.A&, INC-.) ?-q', ' 4`'02 To install, alter, remove, place temporarily out of service or otherwise dispose of any flammable or combustible liquid tank per 79.104 of the Uniform Fire Code. THIS APPLICATION MUST BE RETURNED WITH YOUR CHECK IN THE AMOUNT OF $ , TO THE TUKWILA FIRE DEPARTMENT, 444 ANDOVER PARK EAST, TUKWILA, WASHINGTON, 98188. j bt . ,1 .Q�� sr P'c1717rz JA -c, i N.s` t. L Co) v F./kr-44-- Soo e-44. PXJUL apcuktp -Th-m4 i N 5/20A5- LocA1-70Q�tS �TTzlEtAaiikit. e c r icAu5 P -t' 5-r I NSTa-c.LA1ic4 J NIA -P Cie-45cs- 2m-- T.F.D. Form F.P. 31 PERMIT # 0 FIU.E TUKWILA FIRE DEPARTMENT UNDERGROUND FUEL TANK REMOVAL/INSTALLATION PERMIT RECEIPT # DATE RECEIVED DATE ISSUED CODE REFERENCE: 79.114 F I RM NAME : aLC - EI h/l l`CO>\nviEvo r -A _. FIRM ADDRESS: JOB SITE: PHONE : 2c�p.(dZ3.tipZ NUMBER OF TANKS TO B REMOVE /INSTALLED ( ) Of`L1r T AC.A4 - Dil 1. NAME OF BUSINESS AT JOB SITE: PERSON IN CHARGE: i gE Ft�AcpS3m ([iWtt L) PHONE • 244,.&23.a72-1 12. 1' G'1cttN� A&, I Jc•) 2G& .xd#-. 7602- To 60Z To install, alter, remove, place temporarily out of service or otherwise dispose of any flammable or combustible liquid tank per 79.104 of the Uniform Fire Code. THIS APPLICATION MUST BE RETURNED WITH YOUR CHECK IN THE AMOUNT OF $ TO THE TUKWILA FIRE DEPARTMENT, 444 ANDOVER PARK EAST, TUKWILA, WASHINGTON, 98188. -Z5": . j -cOFQU�" -atAt, 'ro II t isTht-L. (1) c4 - 30o Pa -v>; aRcumo -PrPte. )N SSI✓ Loc -nciv dts -rtt� TeMuIPr . �I �lCP r1c j P -r, moi- E iNs-rpt-GLeencit.1 MAP r7 TANKREMV.PER T.F.D. Form F.P. 31 d'1 _1 Emergency Vent F� rt 4" FPT r J J 2" FPT Normal Vent Opening VENTS Interstitial Tank 4 4" 21" Fs: 12" L 4" FPT 21" �1 6^ 7" 61" l OJb. X11 Height: 49" Weight: 850 lbs. Inner Tank Gauge: 12 Openings are female NPT. Before coating, tank shall be tested and proved tight under a test pressure between 5 and 7 psi. Exterior coating is red iron oxide primer. Tanks shall bear the UL label for Aboveground Doublewall tanks. 2" 2 -- NOTICE THIS PRINT ANO THE INFORMATION CONTAINED HEREIN IS PROPRIETARY TO ACE TANK & EQUIPMENT CO. AND SMALL NOT BE REPRODUCED OR DISCLOSED IN WHOLE OR IN PART. NOR USED FOR ANY DESIGN OR MANUFACTURING PURPOSES, UNLESS AUTHORIZED IN WRITING BY ACE TANK & EOUIPMENT CO. Drawing Is not to scale. Weight & measurements aro approximate. 300 GALLON TANK Part No. AC0030002K1 ABOVEGROUND DOUBLEWALL, UL LISTED i i i 38" 1 Interstitial `T Test Opening Both Sides LIFTING LUG AT CENTERLINE COMER APP • OVAL SIGNATURE 4Le :fir/' £89I-V8Z-90Z'ON 131 7Atil( & CO.EQUIPMENT • HAYWARD P ACE SEATTLE • PORTLAND FOR: itz3if>s<1,, Vt..1 V ll2olJp tEntrAi- JOB: i hoc. , IN L. NOT TO SCALE REQUIRED INVOICE I DATE SALESPERSON COMER APP • OVAL SIGNATURE 4Le :fir/' £89I-V8Z-90Z'ON 131 N GLOBAL ENVIRONMENTAL A Division of Globaal Diving'&lag96 g , Incorporated Mr. Ray Gooding Associated Grocers 3301 South Norfolk Seattle, WA 98168 Dear Mr. Gooding, Global Environmental submits for your records, documentation concerning tank decommissioning at Seattle Plant, Maintenance (Bldg. K) off of East Marginal Way. A narrative report follows with all detailed information concerning, sampling of tank contents, disposal profiles, disposal, tank cutting/cleaning, soil drilling, boring, soil sampling and analytical. Copies of this report should be signed were noted and forward to: 1. Tukwila Fire Department, Mike Alderson, Fire Marshal; 2. Department of Ecology, UST Section; 3. Associated Grocer files for minimum of 5 years. If you have any questions about this information please call me at 206-623-0621 Thank you Global Environmental reg Fladseth Operations Manger 2763 - 13th Avenue S.W. Harbor Island Seattle, Washington 98134 FAX: 206-340-8984 24 hours a day - 206-623-0621 CAssociation of Diving Contractors 0 Spill Control Association of America On April 5, 1995 Global Environmental was called concerning an Underground Storage tank removal. Reportedly, two UST's were removed by Associated Grocer Sub -contractor employed to install a waterline. As the ditch alignment was excavated east along the front of the maintenance shop two UST's were encountered ' near the East end of the South wall. The sub -contractor pumped the contents of the tanks into 15 plastic drums and the empty UST's were removed from the excavation without incident. It is belived the maintenance shop was a dry cleaning shop in past years and the tank were abandoned cleaning solvent tanks. Upon removal of the tanks it was reported that no visibly contaminated soil or unusual odors were noted during the waterline installation or tank removal process. The tanks were located on the south side of the maintenance shop (Building 7) at the Associated Grocers East Marginal Way Facility, 3301 South Norfolk Street, Seattle Washington 98160. The East Marginal Way facility is several acres and the maintenance shop is to the southwest portion of the facility. The area surrounding the tanks is paved and used for container truck storage with several wharehouse and office structures located on the property. TANK AND CONTENTS DISPOSAL Global Environmental was employed to complete the tank decommissioning and to provide closure documentation pursuant to WAC 173-340 Model Toxics Control Act and 173-360 Underground Storage Tank Regulations. A representative sample was taken of the material from each tank by AG personnel and left at the guard shack for pick up by a Global Technician. These samples were delivered to American Laboratory for analysis by laboratory method 8260, closed cup flash point and BTU value. A summary of the results is below. 450 Gallon Tank (Vertical) ANALYTE RESULT (PPM) Acetone 1400 (B) Methylene Chloride 1300 (B) Chloroform 4000 (B) Toluene 1100 m,p, Xylene 900 n-Propylbenzene 700 1,3,5-Trimethylbenzene 700 1,2,4-Trimethylbenzene 2800 s-Butylbenzene 800 FLASH POINT 86 BTU VALUE 19,116 (B) = The compound was found in the method blank ANALYTE 300 Gallon Tank (Horizontal) RESULT PPM) 800 (B) 1000 (B) 3400 (B) < 500 < 500 900 1000 4500 1000 82 20,007 Acetone Methylene Chloride Chloroform Toluene m,p, Xylene n-Propylbenzene 1,3,5-Trimethylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene FLASH POINT BTU VALUE All other compounds listed in the 8260 lab report were below the detection limit of 500 ppm. The compounds Acetone, Methylene Chloride, and Chloroform were present in the lab blank ran with this sample batch. The tank samples showed relatively consistent levels of the same compounds. Therefore these compounds are not believed to be present at the concentrations indicated on the lab report. Based on the above information this material was profiled as Cleaning Solvent with Clean Care Corp. and scheduled for disposal at their permitted waste facility. On April 15, 1996 Global transferred the liquid material from the plastic drums into steel 17H DOT approved containers. The drums were sealed, labeled and staged for disposal of the full steel drums and the empty plastic drums. Sound Testing (Marine Chemists) was on site to inert the tanks with carbon dioxide and approve "Hot Work" prior to cutting the tanks open for cleaning. The decommissioned tanks were loaded and transported to Marine Vacuum Services for further cleaning. All the residual sludge and rinsate material was removed from the tanks and placed into drums. The drummed sludge material was transported to Clean Care by Marine Vacuum Services for final disposal. The cleaned tanks were transported by Global to Seattle Iron and Metal Corp for -- disposal as scrap metal on April 18, 1996. SOIL BORINGS To provide sufficient evidence that the tank did not cause significant contamination and do not pose a threat to human health or the environment, 4 boring were done in the vicinity of the UST's. Please the attached site detail. The borings were advanced with a Hollow Stem Auger to depths not exceeding 15'. Eighteen inch split spoon samples were taken every 2' to 5' for field instrument, visual and/or laboratory analysis. At least one laboratory sample was obtained from each boring. Drill cutting and undisturbed split spoon samples were analyzed using a GAS Tech 201 (hot wire technology) explosive vapor monitor with a PPM function. The instrument was calibrated to 20 ppm Methane as a standard and would respond to field performance testing. Head space samples were obtain by taking random grab soil samples from the drill cuttings or from specific locations from a split spoon soil sample and placing this material in a zip lock bag. Allowing the soil in the bags to stand several minutes prior to reading the vapor concentration in the headspace of the bag. None of the head space samples showed any concentration of explosive vapors. However a slight solvent odor was noted in the mud coming up on the augers from Boring # 3. Therefore laboratory samples were obtained from all split spoon samples retrieved from this boring. Water was encountered at about 10' to 11' in all borings. The borings were sealed at the end of the day with hydrated bentonite chips and the asphalt was repaired with concrete plugs. All the soil generated from this boring project was placed in two 55 gallon drums from disposal at a later date. Please see the table below for a summary of the lab results. VOLATILE B-1@4.5' B-1@9' B-2@4.5' B-2@6' B-2@15' B-3@4.5' B-3@7.5' B-3@10' B-4@6' �_ COMPOUND Chloroform <23 <21 <23 <23 <24 6 J <23 <20 2-Butanone <23 <21 <23 <23 <24 <25 120 <20 Toluene <23 <21 <23 32 <24 <25 <23 <20 Ethylbenzene <23 <21 <23 4 J <24 <25 4 J 51 m,p-Xylene <23 <21 <23 25 <24 <25 <23 130 o -Xylene <23 <21 <23 5 J <24 <25 <23 5 J n-Propylbenzene <23 310 <23 <23 <24 <25 620 1000 1,3,5-Trimethylbenzene <23 <21 <23 <23 <24 <25 <23 410 t-Butylbenzene <23 <21 <23 <23 <24 <25 36 25 1,2,4-Trimethylbenzene <23 360 <23 21 J <24 <25 14 J 1600 s-Butylbenzene <23 <21 <23 <23 <24 <25 350 230 1,3 -Dichlorobenzene <23 <21 <23 <23 <24 <25 6 J <20 1,4 -Dichlorobenzene <23 <21 <23 <23 <24 <25 5 J 6 J 1,2 -Dichlorobenzene <23 <21 <23 <23 <24 <25 65 91 n-Butylbenzene <23 390 <23 <23 <24 <25 120 <20 The highest concentrations of Volatile compounds was in B3 @ 10'. The compounds 1,2,4 - Trimethylbenzene, n - Propylbenzene, 1,3,5 - Trimethylbenzene, were found in the highest concentrations and are consistent with compounds found in the liquid product samples. However the concentrations are very low and do not seem to pose a threat to human health and the environment. Trimethylbenzene is a common constituent to Stoddard Solvent a diesel range type product generally derived from Nonane, Mineral Spirits and Trimethylbenzene. Stoddard Solvent is commonly used as a dry cleaning solvent. To further confirm the material found in the tanks and in B3 was stoddard solvent type constituents the Sample from B3 @ 10' was analyzed for Stoddard Solvent by Laboratory Method WTPH-HCID modified. The result of this analysis was approximately 10 ppm and the chromatagram was consistant with what would be stoddard solvent. Other compounds were detected at lower r � concentrations in this and other borings these concentrations are also low and also do not appear pose a significant threat to human health and the environment. Below is other soil information obtained during the boring investigation B1 @ 3'- 4.5' SOIL DESCRIPTION FROM 3'- 4.5' BLOW COUNTS/6" 6/7/6 SPLIT SPOON RECOVERY 10" Brown Sandy Gravel 4" Brown Fine Sand w/ Silt 2" Brown Med. Fine Sand 4" B1 @ 8'- 9.5' SOIL DESCRIPTION FROM 8'- 9.5' BLOW COUNTS/6" 2/2/3 SPLIT SPOON RECOVERY 18" Brown Fine Sand and Silt 4" Gray Clay 14" B1@9.5'-11' SOIL DESCRIPTION FROM 9.5'- 11' BLOW COUNTS/6" 1/2/3 SPLIT SPOON RECOVERY 18" Gray to Brown Clay 18" B2@3'-4.5' SOIL DESCRIPTION FROM 3'- 4.5' BLOW COUNTS/6" 7/8/8 SPLIT SPOON RECOVERY 8.5" Brown Sandy Gravel 3.5" Brown Sand 5" B2@6'-7.5' SOIL DESCRIPTION FROM 6'- 7.5' BLOW COUNTS/6" 2/3/4 SPLIT SPOON RECOVERY 18" Brown Sand 3" Gray Silty Clay w/ Brown Streaks 15" B2@13.5'- 15' SOIL DESCRIPTION FROM 13.5'- 15' BLOW COUNTS/6" 8/18/21 SPLIT SPOON RECOVERY 14" Gray Clay w/ Organic Material 2" Wet Dark Brown Sand 12" B3 @ 3'- 4.5' SOIL DESCRIPTION FROM 3'- 4.5' BLOW COUNTS/6" 5/6/18 SPLIT SPOON RECOVERY 11" Brown Sandy Gravel 3" Brown Fine Sand w/ Silt 6" Brown Sand 2" B3@6'-7.5' SOIL DESCRIPTION FROM 6'- 7.5' BLOW COUNTS/6" 2/2/4 SPLIT SPOON RECOVERY 17" Brown to Black Sand 3" Brown Organic Silty Sand w/ Clay 2" Gray to Brown Clay 12" B3 @ 9'- 10.5' SOIL DESCRIPTION FROM 9'- 10.5' BLOW COUNTS/6" 2/2/4 SPLIT SPOON RECOVERY 17" Gray to Brown Clay 17" B4@3'-4.5' SOIL DESCRIPTION FROM 3'- 4.5' BLOW COUNTS/6" 6/5/8 " . SPLIT SPOON RECOVERY 9" Pea Gravel 9" B4@6'-7.5' SOIL DESCRIPTION FROM 6'- 7.5' BLOW COUNTS/6" 2/2/3 SPLIT SPOON RECOVERY 17" Brown to Black Sand 2" Brown to Gray Clay 15" B4 @ 9'- 10.5' SOIL DESCRIPTION FROM 9'- 10.5' BLOW COUNTS/6" 1/1/2 SPLIT SPOON RECOVERY 18" Gray to Brown Clay 18" LOCATOR MAPS VICINITY WORK AREAS TANK LOCATIONS AND UTILITIES f 0 WATER LINE NEWLY ASPHALTED AREA 31 • 320 330 0 KJe--P7-44--* vAI\TE\A\CE SHOP • 34 VERTICAL TANK HORIZONTAL TANK ' T ASSOCIATED GROCERS EAST MARGINAL WAY FACILITY PROJECT # 522i BORING LOCATION DETAIL DRAWING # REVISION DRAWN BY ;DATE 1 [7i-5ft-or Z . (V)c_ 1\10122-14-- fderPGr.,P -13-to , LL . . ENVIRONMENTAL WELL REPORT ROJECT NAME: ASSOCIATED GROCERS 411111 ELL IDENTIFICATION NO: A1429 Bl&3 RILLING METHOD: HOLLOW STEM AUGER DRILLER: JOHN AUMIhLER 12244 FIRM: HAYE LING, SIGNATURE CONSULTING' FIRM: GLOBAL ENVIRONMENTAL REPRESENTATIVE: PETE VANDERVELDE AS BUILT START CARD NO: A01970 LOCATION: T 23 R 4E SEC 4 DISTANCE: NE A NE A DATUM: BORING WATER LEVEL ELEVATION: INSTALLED: 04/22/96 DEVELOPED: 04/22/96 DEPTH DRILLED: 9' COMPLETED: 9' WELL DATA FORMATION DESCRIPTION 5' Bentonite -- chips o ' 0 0'-9' Abandoned w/ bentonite chips from bottom up. 0'-1' 1'-6' 6' Gravel fill Brown silty clay Gray silty clay & water ENVIRONMENTAL WELL REPORT CfROJECT NAME: ASSOCIATED GROCERS ELL IDENTIFICATION NO: A1429 B2 RILLING METHOD: HOLLOW STEM AUGER DRILLER: JOHN AUMILLER /2244 FIRM: HAYES DRILL SIGNATURE: CONSULTING TIRM: GLOBAL ENVIRONMENTAL REPRESENTATIVE: PETE VANDERVELDE AS BUILT START CARD NO: A01970 LOCATION: T 23 R 4E SEC 4 DISTANCE: NE g NE x DATUM: BORING WATER LEVEL ELEVATION: INSTALLED: 04/22/96 DEVELOPED: 04/22/96 DEPTH DRILLED:13x' COMPLETED:13x' WELL DATA FORMATION DESCRIPTION 5' 0 Bentonite— chips ci 0'-13x' Abandoned w/ bentonite chips from bottom up. 0'-1' 1'-6' 6'-11' 11' Gravel fill Brown silty clay Gray silty clay & water Gray sand & water ENVIRONMENTAL WELL REPORT OROJECT NAME: ASSOCIATED GROCERS ELL IDENTIFICATION NO: A1429 B4 DRILLING METHOD: HOLLOW STEM AUGER DRILLER: JOHN AUMILLER, #2244 FIRM: HAYE$ -D IL? G, I, SIGNATURE: CONSULTING' FIRM: GLOBAL ENVIRONMENTAL REPRESENTATIVE: PETE VANDERVELDE AS BUILT START CARD NO: A01970 LOCATION: T 23 R 4E SEC 4 DISTANCE: NE NE x DATUM: BORING WATER LEVEL ELEVATION: INSTALLED: 04/22/96 DEVELOPED: 04/22/96 DEPTH DRILLED: 9' COMPLETED: 9' WELL DATA FORMATION DESCRIPTION 5' Bentonite— chips 0 0 0'-9' Abandoned w/ bentonite chips from bottom up. 0'-5' 5'-7' 7' Pea gravel fill Brown silty clay Gray silty clay & water DEPT. OF ECOLOGY FORMS • � -'WASHINGTON STATE DEPARTMENT Of ECOLOGY UNDERGROUND STORAGE TANK 30 DAY NOTICE See back of form for instructions Please E 1 the appropriate box L iIntent Intent to Install to ClosE SITE INFORMATION: Site ID Number (on invoice or available from Ecology if the tank is registered): Site/Business Name: AS' /a -r- e% 6roCCr3 Site Address: 3301 J0u Norfe Str t eej / C- I'V I,/ hy1-00 City ti c/ /j it ti 1 amm TANK INFORMATION TANKS TO.BE CLOSED This section to be filled out`:ONLY if tanks `are being removed Tank ID Projected Tank Substance Date Closure Capacity Stored tank roduct to Date last used Ceaet.>„fit t v� • Is there If no, date tank P the tank? was 0011 t, :9 764� — 7d'002 ZIP-Code TANKS TO BE INSTALLED. This section to be filled out ONLY if tanks are being installed Tank ID Approx. Install Date TANK INSTALLATION TO BE PERFORMED BY (if known): This section to be filled out ONLY if tanks are being installed Service Provider: Contact Name: Telephone. ( ) Address: P.O. Box Street City State ZIP -Code TANK PERMANENT CLOSURE TO BE PERFORMED BY (if known): Service Provider Contact Name Telephone: :Address: This section to be --filled out ONLY if tanks care being removed %Pei Tlar'J7 I t>l�J < t ag i7� street 'ZiP-Code::;: This form will be returned to this address UST OWNER/ e /� - : 'ate Ore Cr -if OPERATOR r� C'6 i:�sb 7 / ADDRMAILINEG 33D! 60,,;/17/6d�'r-/!l 5/ ee-/ Street 3e4/ 11.454 Zki City State / ZIP -Code Please type or print information Once validated by Ecology, this form serves as your temporary permit for the tanks listed above. ECY 020-33 UNDERGROUND STORAGE TANK TEMPORARY/PERMANENT CLOSURE and SITE ASSESSMENT NOTICE See back of form for instructions WASHINGTON STATE I✓' OEPARTHENT OF Please r- � the appropr to box(es) Please type or print informatio Temporary 1_1Tank Closure ECOLOGY Permanent Closure Service Change-In- ite Assessment/ Site Check SITE INFORMATION: Site ID Number (on invoice or available from Ecology if the tanks are registered). i Site/Business Name- .45,50c- icfe'c( 6,0c e✓s- Site Address: 330 1 Sou -i-1 de/fd/ir Street el c y k�41/:�Tn�t 101‘6 ccs S-76 Telephone: ( (2a ) 764---ZPr'7rc2 State ZIP -Code TANK INFORMATION: CONTAMINATION Tank ID Closure Date Lf-p2--Mso/,-/-,,,,..,,,.1..5.,11,./- Tank Capacity Substance Stored PRESENT AT THE TINE. OF CLOSURE LI LI Yes No et P; -/!C 306 C[ e.Z n, S0,-,:t27` . ^ ,-1 Supervisors Signature: /L/� -e.0..../- _ // Address- )76 ✓ 13i4 Nvc=✓1 ,E c .0W.7g414-5 / Unknown Check unknown obvious contamination observed results have received from [[�� Street/ ', // f1 3C 11`el bia' :1- ktdi, 11.h_5h/h,ci if no was yet been lab. D r 7 friIQ ZIP -Code City Telephone- ( 2' ‘-'�� - fi ' -2- / and sample not analytical SITE CHECK/SITE ASSESSMENT CONDUCTED//BY: Name of Registered Site Assessor: P - C Vito c VVCtJe. Telephone: (o6,) ;49 -6-)30 /366/ 1 E SaKAI-_/ / - 3 Address �p N.�.`cE' UST SYSTEM OWNER/OPERATOR:. . ec5 p l Zone- ( b�) 70 — 7OQt UST Owner/Operator �c cc SOC 41111. Owners Signature: c� Q i Address: 3301 6-64 /A /YC✓ra[ K ,,, /vec- 71'- tr et , 4sil/'17�/0•/ �-itot , 1,45e P.O. Box fY/66 City State ZIP -Code TANK CLOSURE/CHANGE-IN-SERVICE PERFORMED BY: Service Provider: 6701, / C rr►✓/rem bs1 P•t 1L4Z r License Number -50O11)-it Licensed Supervisor Gr Cy Phd s c- fil LLiiceonse Number: lie_ ( xv £Z?G'7 / . ^ ,-1 Supervisors Signature: /L/� -e.0..../- _ // Address- )76 ✓ 13i4 Nvc=✓1 ,E c .0W.7g414-5 / [[�� Street/ ', // f1 3C 11`el bia' :1- ktdi, 11.h_5h/h,ci P.O. Box State D r 7 friIQ ZIP -Code City Telephone- ( 2' ‘-'�� - fi ' -2- / SITE CHECK/SITE ASSESSMENT CONDUCTED//BY: Name of Registered Site Assessor: P - C Vito c VVCtJe. Telephone: (o6,) ;49 -6-)30 /366/ 1 E SaKAI-_/ / - 3 Address �p N.�.`cE' �y A - /Street j��1/r e waS5tr1ltk4/c f qy/%6 P.O. Box State ZIP -Code City / ECY 020-34 UNDERGROUND STORAGE TANK ,,,,,,i1II 1,,,, Site Check/Site Assessment Checklist lrrIliut+T or ,ECOLOGY Owner # For Office Use Only INSTRUCTIONS: When a release has not been confirmed and reported, this Site Check/Site Assessment Checklist must be completed and signed by a person registered with the Department of Ecology. The results of the site check or site assess- ment must be included with this checklist. This form must be submitted to Ecology at the address shown below within 30 days after completion of the site check/site assessment. SITE INFORMATION: Include the Ecology site ID number if the tanks are registered with Ecology. This number may be found on the tank owner's invoice or tank permit. TANK INFORMATION: Please list all the tanks for which the site check and site assessment is being conducted. Use the tank ID number if available, and indicate tank capacity and substance stored. REASON FOR CONDUCTING SITE CHECK/SITE ASSESSMENT: Please check the appropriate item. CHECKLIST: Please initial each item in the appropriate box. SITE ASSESSOR INFORMATION: This form must be signed by the registered site assessor who is responsible for conducting the site check/ site assessment. Underground Storage Tank Section Department of Ecology P. O. Box 47655 Olympia, WA 98504-7655 SITE INFORMATION Site ID Number (on invoice or available from Ecology if the tanks are registered): Site/Business Name: 4 SS oc, `aicc/ 6w6 c. •°S Site Address: 33t)/ 5614-f17NOrfo`/t 574-crj Telephone: I Street %�.-0,4 City Y/60 State ZIP -Code TANK INFORMATION Tank ID No. /Tank Capacity TSo ��I��nt IOC' �c�/lt�Hseq Substance Stored REASON FOR CONDUCTING SITE CHECK/SITE ASSESSMENT Check one: Investigate suspected release due to on-site environmental contamination. Investigate suspected release due to off-site environmental contamination. Extend temporary closure of UST system for more than 12 months. UST system undergoing change -in-service. UST system permanently closed -in-place. UST system permanently closed with tank removed. Abandoned tank containing product. Required by Ecology or delegated agency for UST system closed before 12/22/88. Other (describe): ECY 010-158 page 1 CHECKLIST YES O Each item of the following checklist shall be initialed by the person registered with the Department of Ecology whose signature appears below. i is shown on the vicinitymap. 1. The location of the UST site p 2. A brief summary of information obtained during the site inspection is provided, (see Section 3.2 in the Site Assessment Guidance) v 3. • A summary of UST system data is provided. (see Section 3.1) / !� 4. The soils characteristics at the UST site are described. (see Section 5.2) 1/ 5. Is there apparent groundwater in the tank excavation? 6. A brief description of the surrounding land is provided. (see Section 3.1) 7. Information has been provided indicating the number and types of samples collected, methods used to collect and analyze the samples, and the name and address of the laboratory used to perform the analyses. t/ - 8. A sketch or sketches showing the following items is provided: - location and ID number for all field samples collected 1 / - groundwater samples distinguished from soil samples (if applicable) • 1 - samples collected from stockpiled excavated soil - tank and piping locations and limits of excavation pit ,J - adjacent structures and streets -approximate locations of any on-site and nearby utilities 9. If sampling procedures different from those specified in the guidance were used, has . justification for using these alternative sampling procedures been provided? (see Section 3.4) / 10. A table is provided showing laboratory results for each sample collected including: sample ID number, constituents analyzed for and corresponding concentration, analytical method and detection limit for that method. 7 11. Any factors that may have compromised the quality of the data or validity of the results are described. 12. The results of this site check/site assessment indicate that a confirmed release of regulated substance has occured. / SITE ASSESSOR INFORMATION All F'cfc aka e✓✓cid e 6104/ Ever..%t.11e-z PERSON REGISTERED WITH ECOLOGY FIRM AFFILIATED WITH ATELEPHONE:(2 a V 9 ^67 Sd BUSINESS ADDRESS: / 30 'I/ a 14 4v ��K C 54/ 6C411//a 144 54,, fere 4d'/i. CITY STATE ZIP+CODE I hereby certify that I have been in responsible charge of performing the site check/site assessment described above. Persons submitting false information are su ject to penalties under Chapter 173-360 1VAC..5706 ��'t- Date Signature of Person Registered with Ecology FIRE DEPT. PERMITS MARINE CHEMIST CERTS SOUND TESTING. INC. P.O. BOX 16204 SEATTLE, WA 98116 (206) 932-0206 CNV 1 i da.vl ca. rn-t., Requested by a l:Sr #9- "G`5 MARINE CHEMIST CERTIFICATE SERIAL N? 43044 is Are 96 i %C,C, j Aim Gac Cd S Vessel Owner or Agent S'r' Vessel U <, SCC -VC.,., Last Three 13) Cargoes Date AsSoe, C,2cc ,.c aL Type of Vessel Specific Location of Vessel - Ci 2 I % Ski A1� T" Test Metlriod Time Survey Completed u S -i 's - S 4 -FE e., {--tc T. Uljo e,cC . e I N 6_4.i J 5 ! C.4 N ry i ►J L. E �S 1— cue '-oc . I'J ./(2.•nri4eA2 t tk3044e i°bcu r1- 4- i Zco In the event of any physical or atmospheric changes adversely affecting the gas -free condition of the above spaces, or if In any doubt, immediately stop all work and contact the undersigned Marine Chemist QUAUFICATSON$: Transfer of ballast or manipulation of valves or closure equipment tending to after conditions in pipe erns, tanks or compartments subject to gas accumulation, tintless specifically approved in this Certificate, requires inspection and endorsement or reissue of CsrtMcate for the spaces so affected. All lines, vents, heating coils, valves, end similarly enclosed appurtenances shall be considered "not safe" unless otherwise specifically designated. STANDARD SAFETY DESIGNATIONS SAFE FOR WORKERS. Means that in the compartment or space so designated Lal the oxygen content of the atmosphere is at least 19.5 percent by volume, and that. OA toxic materials in the atmosphere are within permissible concentrations, and that. (c► the residues are not capable of producing toxic materials under existing atmospheric conditions while maintained as directed on the Marine Chemist's Certificate. NOT SAFE FOR WORKERS. Means that in the compartment or space so designated. the requirements of Safe for Workers has not been met. SAFE FOR HOT WORK: Means that in the compartment so designated: la) oxygen content of the atmosphere is at least 19.5 percent by volume, with the exception of inertedspaces or where external hot work is to be performed; and that. Ib) the concentration of flammable materials in the atmosphere is below 10 percent of the lower flammable limit; and that. Icl the residues are not capable of producing a higher concentration than permitted by Ib) above under existing atmospheric conditions in the presence of fire, and while maintained as directed on the Marine Chemist's Certificate; and further, that, (dl all adjacent spaces have been cleaned sufficiently to prevent the spread of fire, or are satisfactorily inerted, or, in the case of fuel tanks, or lube oil tanks, or engine room or fire room bilges, have been treated in accordance with the Marine Chemist's requirements. NOT SAFE FOR HOT WORK. Meansaat in the compartment so designated, the requirements of Safe for Hot Work have not been met SAFE FOR REPAIR YARD ENTRY Means that the compartments and spaces of the flammable cryogenic liquid carrier so designated: (a) have been tested by sampling at remote sampling stations, and results indicate the atmosphere tested to be above 19.5 percent oxygen, and less than 10 percent of the lower flammable limit, or (b) are alerted CHEMIST'S ENDORSEMENT This is to certify that I have personally determined that all spaces in the foregoing list are in accordance with NFPA306-1980Control of Gas QHHazards on Vessels and have found the condition of each to be in accordance with its assigned designation. undersigned acknowledges receipt of this Certificate under Section 2-3 of NFPA 306-1980 This Certificate is based on conditions existing at the tune the inspection herein set and understands conditions and limitations under which it was issued " forth was completed and is issued s blect to c • hence with all qualifications and instructions , �_ Signed (4-1Q- ct Nem* Comeenr VESSEL POSTING ate Signed DISPOSAL RECEIPTS WATER, OIL, TANKS 0 J1 10 Y ` n 0 1 GLOBAL DIVING 318990 SEATTLE IRON & METALS CORP. 2955 11th AVE S.W., P.O. BOX 3793 • SEATTLE, WASHINGTON 98124 (206) 682-0040 • FAX: (206) 623-1231 dealers and brokers... .} MON AND STEEL SCRAP • NON-FERROUS METALS . STEEL PRODUCTS • DISMANTLERS • NUMBER DESCRIPTION • ''WEIGHT 4/18/96 DATE11:07 AM 062 RECEIPT NUMBER: ?PREPARED PRICE AMOUNT 3545 #2 UhPREP RED h ` x. - , t PA I -D • Dq 181776 SEATTLE IRON &,METALS CORP. 1640 35.0000/NT 28.70 TOTAL: 28.70 I hereby certify that I am the lawful owner of the merchandise listed above, and that this merchandise is free of encumbrances, and that I am of legal age. I also certify that the weights shown abpve are c • _ .' and fin = anc�,receipt of the amount shown above is hereby acknowledged in full payment for the merchandise f am sel X(J ACCEPTED: ANALYTICAL REPORTS 0 AMERICAN ANALYTICAL LABORATORIES, INC. April 12, 1996 Global Environmental 2763 13th Ave SW, Harbor Island Seattle, WA 98134 Attn.: Greg Fladseth Dear Greg: Enclosed are the results of the analyses of samples submitted on 4/08/96 from your Associate Grocerys Project. We appreciate the opportunity to be of service to you on this project. If you have any questions regarding the reported results, please feel free to call me. Sincerely, Todd Saamonsen� Laboratory Director enclosures AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�� 0 Date of Analysis: 4/12/96 Samples Submitted: 4/8/96 File ID: 04-029 Analysis: Flash Point Units: Degrees Fahrenheit Client: Global Environmental Project: Associate Grocerys Project #: Matrix: Liquid Lab ID Client ID Result 04-029-1 04-029-2 450 Gallon 300 Gallon 86 82 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 0 Date of Analysis: 4/12/96 Samples Submitted: 4/8/96 File ID: 04-029 Analysis: BTU Units: BTU/lb. Client: Global Environmental Project: Associate Grocerys Project #: Matrix: Liquid Lab ID Client ID Result 04-029-1 04-029-2 450 Gallon 300 Gallon 19,116 20,007 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 D 0 0 Sample # 300 Gal Method: Analyst Matrix: Sample (ml): Extract (m1): Sparge (ul): EPA 8260 AALI>IF 04-029-2 T. Meadows Data File: C:IHPCHEMl1IDATA19604101 2901011.D Liquid Instrument GCMS1 0.05 Extraction: 04110196 5.0 Analysis: 04110196 5.0 Surrogates Recovery Limits Dibromofluoromethane 111% 74.121 Toluene -d8 100% 80-120 4-Bromofluorobenzene 115% 81-117 Target Analytes Concentration (ppm) Chloromethane 500 U Vinyl Chloride 500 U Bromomethane 500 U Chloroethane 500 U Trichlorofluoromethane 500 U 1,1-Dichloroethene 500 U Acetone 800 B Methylene Chloride 1,000 B cis-1,2-Dichloroethene 500 U trans•1,2•Dichloroethene 500 U 1,1-Dichloroethane 500 U Bromochloromethane 500 U Chloroform 3,400 B 2-Butanone (MEK) 500 U 1,1,1 -Trichloroethane 500 U 1,1-Dichloropropene 500 U 1,2•Dichloroethane 500 U Carbon Tetrachloride 500 U Benzene 500 U Trichloroethene 500 U 1,2-Dichloropropane 500 U Dibromomethane 500 U Bromodichloromethane 500 U cis-1,3-Dichloropropene 500 U trans-1,3-Dichloropropene 500 U 1,1,2 -Trichloroethane 500 U Dibromochloromethane 500 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J • Tenatively Identified at a level below normal detection limits. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 0 Data File: Sample #: 300 Gal cont. C:IH PCH EMI I IDATA19604101 Target Analytes cont. 4-Methyl-2-Pentanone (MIRK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2•Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5•Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene 2901011.D Data Qualifiers B • The compound was found in the method blank. Q • Excedes the Quality control limits. U - The compound was not detected. J • Tenatively Identified at a level below normal detection limits. Concentration (ppm) 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 900 500 U 1,000 500 U 500 U 4,500 1,000 500 U 500 U 500 U 500 U AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA98108 ish Page 2 of 2 0 Sample A 450 Gal Method: Analyst Matrix: Sample (ml): Extract (ml): Sparge (ul): EPA 8260 AALIAF 04-029-1 T. Meadows Data File: C:IHPCHEMIIIDATAI9604101 2801010.D Liquid Instrument: GCMS1 0.05 Extraction: 04110196 5.0 Analysis: 04110196 5.0 Surrogates Recovery Limits Dibromofluoromethane 93% 74-121 Toluene -d8 98% 80-120 4-Bromofluorobenzene 100% 81-117 Target Analytes Concentration (ppm) Chloromethane 500 U Vinyl Chloride 500 U Bromomethane 500 U Chloroethane 500 U Trichlorofluoromethane 500 U 1,1-Dichloroethene 500 U Acetone 1,400 B Methylene Chloride 1,300 B cis-1,2-Dichloroethene 500 U trans-1,2-Dichloroethene 500 U 1,1-Dichloroethane 500 U Bromochloromethane 500 U Chloroform 4,000 B 2•Butanone(MEK) 500 U 1,1,1 -Trichloroethane 500 U 1,1-Dichloropropene 500 U 1,2-Dichloroethane 500 U Carbon Tetrachloride 500 U Benzene 500 U Trichloroethene 500 U 1,2-Dichloropropane 500 U Dibromomethane 500 U Bromodichloromethane 500 U cis-1,3-Dichloropropene 500 U trans-1,3-Dichloropropene 500 U 1,1,2 -Trichloroethane 500 U Dibromochloromethane 500 U Data Qualifiers B • The compound was found in the method blank. Q . Excedes the Quality control limits. U - The compound was not detected. J . Tenatively Identified at a level below normal detection limits. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 Sample #: Method Blank cont. 0 Data File: 0 C:IHPCHEM111DATA19604101 Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2•Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2•Hexanone (MBK) Chlorobenzene Ethylbenzene m,p•Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n•Propylbenzene 2•Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene 1901003.D Data Qualifiers B . The compound was found in the method blank. Q - Excedes the Quality control limits. U • The compound was not detected. J . Tenatively Identified at a level below normal detection limits. Concentration (ppm) 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 io Page 2 of 2 0 a Sample #: Laboratory Control Spike Method: Analyst Matrix: Sample (ml): Extract (ml): Sparge (ul): EPA 8260 T. Meadows Blank 0.05 5.0 5.0 Surrogates Recovery Limits AALIM 4110196-LCS Data File: C:IHPCHEMI1IDATAI9604101 2001004.0 Instrument GCMS1 Extraction: 04110196 Analysis: 04110196 Dibromofluoromethane 109% Toluene -d8 94% 4-Bromofluorobenzene 90% 74-121 80-120 81-117 Target Analytes Recovery(%) Limits 1,1-Dichloroethene 98% 50-150 Benzene 117% 50-150 Trichloroethene 103% 50-150 Toluene 111% 50-150 Chlorobenzene 108% 50.150 Data Qualifiers Q • Excedes the Quality control limits AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 0 Sample #: 300 Gal Duplicate Method: Analyst Matrix: Sample (mil: Extract (ml): Sparge (ul): EPA 8260 AALl#: 04-029-2 Dup T. Meadows Data File: C:IHPCHEMIIIDATAI9604101 3001012.0 Liquid Instrument: GCMS1 0.05 Extraction: 04111196 5.0 Analysis: 04111196 5.0 Surrogates Recovery Limits Dibromofluoromethane 111% 74.121 Toluene -d8 102% 80-120 4-Bromofluorobenzene 115% 81.117 Target Analytes Concentration (ppm) Chloromethane 500 U Vinyl Chloride 500 U Bromomethane 500 U Chloroethane 500 U Trichlorofluoromethane 500 U 1,1-Dichloroethene 500 U Acetone 600 B Methylene Chloride 1,000 B cis-1,2-Dichloroethene 500 U trans-1,2-Dichloroethene 500 U 1,1-Dichloroethane 500 U Bromochloromethane 500 U Chloroform 3,400 B 2-Butanone (MEK) 500 U 1,1,1 -Trichloroethane 500 U 1,1-Dichloropropene 500 U 1,2-Dichloroethane 500 U Carbon Tetrachloride 500 U Benzene 500 U Trichloroethene 500 U 1,2-Dichloropropane 500 U Dibromomethane 500 U Bromodichloromethane 500 U cis-1,3-Dichloropropene 500 U trans-1,3-Dichloropropene 500 U 1,1,2 -Trichloroethane 500 U Dibromochloromethane 500 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - Tenatively Identified at a level below normal detection limits. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 Sample # 300 Gal Duplicate Data File: cont. C:IHPCHEMIIIDATA19604101 Target Analytes cont. 4•Methyl-2•Pentanone (MIRK) Toluene 1,2•Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2•Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5•Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene 3001012.D Data Qualifiers B • The compound was found in the method blank. Q . Excedes the Quality control limits. U - The compound was not detected. J . Tenatively Identified at a level below normal detection limits. Concentration (ppm) 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 500 U 1,000 500 U 1,000 500 U 500 U 4,900 1,100 500 U 500 U 500 U 500 U AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 ANALYTICAL LABORATORIES, INC. Client Name Project Name 7/ 550 C, i'1 /� ���GG /LYS • Project No. PO No. (206) 762-7599 FAX (206) 762-7665 8220 7th Avenue South Seattle, WA 98108 --/c775 c - CHAIN -OF -CUSTODY / REQUEST FOR OALYSIS 04 04 Batch Send Lab Report To Date Required /00,2 "4-1. Client Contact Client Contact Phone Analysis Requested Number Sample I.D. Date Collected Time Collected Matrix Sample Number of Containers // / / / / / / /Comments / 41509-L y4I6oC) 1 x ..5 ov .2,y C. yl-% 15o0 , K Special Instructions .times L 47rZi 00,-,ES:54/ Was Preservative Used? N • O Yes 7 ' at Kind? 1. Relinquished By - Dateqe- 76 Time /5 /a Received By C/ 2. Relinquished By Date Time What Anaalysis? oj Date f -9G Time l Received By Date Time AMERICAN ANALYTICAL LABORATORIES. INC. April 25, 1996 Global Environmental 2763 13th Ave SW, Harbor Island Seattle, WA 98134 Attn: Greg Fladseth Dear Greg: Enclosed are the results of the analyses of samples submitted on 4/22/96 from your AG Project. ® We appreciate the opportunity to be of service to you on this project. If you have any questions regarding the reported results, please feel free to call me. Sincerely, Laboratory Director enclosures • AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Narrative for batch 04-063 0 T. Meadows 04/26/96 Method: 8260 The recovery of the surrogate Toluene -d8 for sample 04-063-7 (B-3 @ 4.5) was below the control limits. Since the recoveries of the other two surrogates were in control no further action is recommended. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 0 • Sample #: Method Blank Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Blank 1.0 5.0 5.0 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1 ,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis -1, 3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 4/24/96 -MB Data File: C:\HPCHEM\1\DATA\960424\ 1901003.D Instrument: GCMS1 Extraction: 04/24/96 Analysis: 04/24/96 Recovery 96% 93% 93% Data Qualifiers B - The compound was found in the method blank. ® Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report Limits 74-121 80-120 81-117 Concentration (ppb) 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U level. The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�i Sample #: Method Blank cont. 11) Data File: 0 C:\HPCHEM\1\DATA\960424 1901003.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3, 5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 0 et 0 Sample #: Laboratory Control Spike Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Blank 1.00 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes 1,1-Dichloroethene Benzene Trichloroethene Toluene Chlorobenzene AALI#: Data File: Instrument: Extraction: Analysis: Recovery 102% 99% 96% Recovery(%) 100% 102% 95% 99% 100% 4/24/96-LCS C:\HPCHEM\1\DATA\960424\ 2001004.D GCMS1 04/24/96 04/24/96 Limits 74-121 80-120 81-117 Limits 50-150 50-150 50-150 50-150 50-150 Data Qualifiers Q - Excedes the Quality control limits AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�� Sample #: B-1 @ 4.5 Method: EPA 8260 AALI#: 04-063-1 Analyst: T. Meadows Data File: C:\HPCHEM\1\DATA\960424I 21O1OO5.D Matrix: Soil Instrument: GCMS1 Sample (gm): 1.1 Extraction: 04/24/96 Extract (ml): 5.0 Analysis: 04/24/96 Sparge (ml): 5.0 Surrogates Recovery Limits Dibromofluoromethane 105% 74-121 Toluene -d8 100% 80-120 4-Bromofluorobenzene 99% 81-117 Target Analytes Concentration (ppb) Chloromethane 23 U Vinyl Chloride 23 U Bromomethane 23 U Chloroethane 23 U Trichlorofluoromethane 23 U 1,1-Dichloroethene 23 U Acetone 23 U Methylene Chloride 23 U cis-1,2-Dichloroethene 23 U trans-1,2-Dichloroethene 23 U 1,1-Dichloroethane 23 U Bromochloromethane 23 U Chloroform 23 U 2-Butanone (MEK) 23 U 1,1,1 -Trichloroethane 23 U 1,1-Dichloropropene 23 U 1,2-Dichloroethane 23 U Carbon Tetrachloride 23 U Benzene 23 U Trichloroethene 23 U 1,2-Dichloropropane 23 U Dibromomethane 23 U Bromodichloromethane 23 U cis-1,3-Dichloropropene 23 U trans-1,3-Dichloropropene 23 U 1,1,2 -Trichloroethane 23 U Dibromochloromethane 23 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Sample #: B-1 @ 4.5 cont. eData File: C:\HPCHEM\1\DATA\960424 21O1005.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U Data Qualifiers B - The compound was found in the method blank. Q -Excedes the Quality control limits. u_ The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�i 0 • Sample #: B-1 @ 4.5 Duplicate Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.0 5.0 5.0 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-1 Dup Data File: C:\HPCHEM\1\DATA\960424\ 2301006.D Instrument: GCMS1 Extraction: 04/24/96 Analysis: 04/24/96 Recovery 98% 95% 95% Limits 74-121 80-120 81-117 Concentration (ppb) Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�� Sample #: B-1 @ 4.5 Duplicate cont. Data File: C:\HPCHEM\1\DATA\960424 2301OO6.D Target Analytes cont. 4-Methyl-2-Pentanone (MIRK) Toluene 1, 2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1, 2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U Data Qualifiers B - The compound was found in the method blank. Q -Excedes the Quality control limits. u_ The compound wasnot detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� • Sample #: B-1 @ 4.5 Matrix Spike Method: EPA 8260 AALI#: 04-063-1 MS Analyst: T. Meadows Data Fie: C:\HPCHEM\1\DATA\960424\ 24O1O07.D Matrix: Soil Instrument: GCMS1 Sample (gm): 1.05 Extraction: 04/24/96 Extract (ml): 5.00 Analysis: 04/24/96 Sparge (ml): 5.00 Surrogates Recovery Limits Dibromofluoromethane 116% 74-121 Toluene -d8 99% 80-120 4-Bromofluorobenzene 102% 81-117 Target Analytes Recovery(%) Limits 1,1-Dichloroethene 98% 50-150 Benzene 111% 50-150 Trichloroethene 113% 50-150 Toluene 107% 50-150 Chlorobenzene 108% 50-150 Data Qualifiers Q - Excedes the Quality control limits AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 0 • • Sample #: B-1 @ 9.5 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.18 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEI() 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-2 Data File: C:\HPCHEM\1\DATA\960424\ 2501008.D Instrument: GCMS1 Extraction: 04/24/96 Analysis: 04/24/96 Recovery 110% 93% 111% Limits 74-121 80-120 81-117 Concentration (ppb) 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 i�� Sample #: B-1 @ 9.5 cont. Data File: C:\HPCHEM\1\DATA\960424 25O10O8.D Target Analytes cont. 4-Methyl-2-Pentanone (MIRK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3, 5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1, 2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 21 U 310 21 U 21 U 21 U 21 U 24 360 21 U 21 U 21 U 390 Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� Sample #: B-2 © 4.5 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.11 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1, 2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-3 Data File: C:\HPCHEM\1\DATA\960424\ 2601009.D Instrument: GCMS1 Extraction: 04/24/96 Analysis: 04/24/96 Recovery 107% 97% 98% Limits 74-121 80-120 81-117 Concentration (ppb) 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U Data Qualifiers B - The compound was found in the method blank. Q -Excedes the Quality control limits. • u_ The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 Sample #: B-2 @ 4.5 cont. • Data File: • C:\HPCHEM\1\DATA\960424 2601009.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U Data Qualifiers B - The compound was found in the method blank. Q -Excedes the Quality control limits. • u_ The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� 0 Sample #: B-2 @ 6.0 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 AALI#: 04-063-4 T. Meadows Data File: C:\HPCHEM\1 \DATA\960424\ 28O1O1O.D Soil Instrument: GCMS1 1.1 Extraction: 04/25/96 5.0 Analysis: 04/25/96 5.0 Surrogates Recovery Limits Dibromofluoromethane 119% 74-121 Toluene -d8 93% 80-120 4-Bromofluorobenzene 101% 81-117 Target Analytes Concentration (ppb) Chloromethane 23 U Vinyl Chloride 23 U Bromomethane 23 U Chloroethane 23 U Trichlorofluoromethane 23 U 1,1-Dichloroethene 23 U Acetone 23 U Methylene Chloride 23 U cis-1,2-Dichloroethene 23 U trans-1,2-Dichloroethene 23 U 1,1-Dichloroethane 23 U Bromochloromethane 23 U Chloroform 23 U 2-Butanone (MEK) 23 U 1,1,1 -Trichloroethane 23 U 1,1-Dichloropropene 23 U 1,2-Dichloroethane 23 U Carbon Tetrachloride 23 U Benzene 23 U Trichloroethene 23 U 1,2-Dichloropropane 23 U Dibromomethane 23 U Bromodichloromethane 23 U cis-1,3-Dichloropropene 23 U trans-1,3-Dichloropropene 23 U 1,1,2 -Trichloroethane 23 U Dibromochloromethane 23 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 • • Sample #: B-2 @ 6.0 cont. Data File: C:\HPCHEM\1\DATA\960424 28O1O1O.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1, 2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 23 U 32 23 U 23 U 23 U 23 U 23 U 23 U 4 J 25 5 J 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 21 J 23 U 23 U 23 U 23 U 23 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 Sample #: B-2 @ 15 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.04 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-6 Data File: C:\HPCHEM\1\DATA\960424\ 2901011.D Instrument: GCMS1 Extraction: 04/25/96 Analysis: 04/25/96 Recovery 116% 91% 98% Limits 74-121 80-120 81-117 Concentration (ppb) Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�� Sample #: B-2 @ 15 cont. le Data File: C:\HPCHEM\1 \DATA\960424 2901011.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U 24 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. ®U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� 0 e Sample #: B-3 @ 4.5 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.00 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: Data File: Instrument: Extraction: Analysis: Recovery 117% 38% 91% 04-063-7 C:\HPCHEM\1\DATA\960424\ 3001012.D GCMS1 04/25/96 04/25/96 Q Limits 74-121 80-120 81-117 Concentration (ppb) Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. ® U - The compound was not detected. J - The compound was detected below the normal report level. 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 6 J 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Sample #: B-3 @ 4.5 cont. 11, Data File: 0 C:\HPCHEM\1\DATA\960424 30O1012.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1, 2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U 25 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� 0 Sample #: B-3 @ 7.5 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.08 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: Data File: Instrument: Extraction: Analysis: Recovery 92% 98% 87% 04-063-8 C: \H PCH EM\ 1 \DATA\960424\ 3701015.D GCMS1 04/25/96 04/25/96 Limits 74-121 80-120 81-117 Concentration (ppb) Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 120 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U The amount is an estimate. Page 1 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 i�� Sample #: B-3 @ 7.5 cont. Data File: C:\HPCHEM\1\DATA\960424 3701O15.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 23 U 23 U 23 U 23 U 23 U 23 U 23 U 23 U 4 J 23 U 23 U 23 U 23 U 23 U 620 23 U 23 U 23 U 36 14 J 350 6 J 5 J 65 120 Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of 2 i�� 0 Sample #: B-3 @ 10.0 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.22 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-9 Data File: C:\HPCHEM\1\DATA\960424\ 3801016.D Instrument: GCMS1 Extraction: 04/25/96 Analysis: 04/25/96 Recovery 96% 105% 92% Limits 74-121 80-120 81-117 Concentration (ppb) 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 Sample #: B-3 @ 10.0 cont. Data File: C:\HPCHEM\1\DATA\960424 38O1O16.D Target Analytes cont. 4-Methyl-2-Pentanone (MIBK) Toluene 1 ,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1 ,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1,2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 20 U 20 U 20 U 20 U 20 U 20 U 20 U 20 U 51 130 5 J 20 U 20 U 20 U 1,000 20 U 410 20 U 25 1,600 230 20 U 6 J 91 20 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. Page 2 of 2 AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 C • Sample #: B-4 @ 6.0 Method: Analyst: Matrix: Sample (gm): Extract (ml): Sparge (ml): EPA 8260 T. Meadows Soil 1.47 5.00 5.00 Surrogates Dibromofluoromethane Toluene -d8 4-Bromofluorobenzene Target Analytes Chloromethane Vinyl Chloride Bromomethane Chloroethane Trichlorofluoromethane 1,1-Dichloroethene Acetone Methylene Chloride cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,1-Dichloroethane Bromochloromethane Chloroform 2-Butanone (MEK) 1,1,1 -Trichloroethane 1,1-Dichloropropene 1,2-Dichloroethane Carbon Tetrachloride Benzene Trichloroethene 1,2-Dichloropropane Dibromomethane Bromodichloromethane cis-1,3-Dichloropropene trans-1,3-Dichloropropene 1,1,2 -Trichloroethane Dibromochloromethane AALI#: 04-063-10 Data File: C:\HPCHEM\1 \DATA\960424\ 39O1017.D Instrument: GCMS1 Extraction: 04/25/96 Analysis: 04/25/96 Recovery 78% 104% 92% Limits 74-121 80-120 81-117 Concentration (ppb) 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 1 of 2 i�� Sample #: B-4 @ 6.0 cont. Data File: C:\HPCHEM\1\DATA\960424 39O1O17.D Target Analytes cont. 4-Methyl-2-Pentanone (MIRK) Toluene 1,2-Dibromoethane 1,1,1,2 -Tetrachloroethane Bromoform Tetrachloroethene 2-Hexanone (MBK) Chlorobenzene Ethylbenzene m,p-Xylene o -Xylene Styrene Bromobenzene 1,1,2,2 -Tetrachloroethane n-Propylbenzene 2-Chlorotoluene 1,3,5-Trimethylbenzene 4-Chlorotoluene t-Butylbenzene 1, 2,4-Trimethylbenzene s-Butylbenzene 1,3 Dichlorobenzene 1,4 Dichlorobenzene 1,2 Dichlorobenzene n-Butylbenzene Concentration (ppb) 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 17 U 18 17 U 17 U 17 U 6 J 7 J 51 17 U 17 U 6. J 17 U Data Qualifiers B - The compound was found in the method blank. Q - Excedes the Quality control limits. U - The compound was not detected. J - The compound was detected below the normal report level. The amount is an estimate. AMERICAN ANALYTICAL LABORATORIES, INC. (206) 762-7599 / FAX (206) 762-7665 / 8220 7th Avenue South / Seattle, WA 98108 Page 2 of.2 i�i • 7 V) oo 7O 4 s3 4 N co co Send Lab Report To U z 74 41 o F a o J -a U_ F z Client Name 6Z)- 06.2/ • L a) 1 E aS O Z Z m 0 'o 0 a 0.. d Z 0 a r+• n v Client Contact / `` `/ / / / / / / / Comments I Number of Containers — , •— — — — Time Collected Sample I.D. in 11O ® ` Q ci il CZ) ri iI) g r{ to 'b) ci * 1'9 r'1 in, t \ r ®'Ci r1 it O, ttcl Qi V- U V a� a) E E F= H CD >5CIO • m 'O V .2 CC CC Q) rt \, V Special Instructions 1. Relinquished By E p a) at Q 2. Relinquished By Narrative for batch 04-063 T. Meadows 05/08/96 Method: WTPH-HCID The sample 04-063-9 (B-3@10) had a chromatographic pattern similar to that of our Stoddard Solvent standard. The area of this pattern was well below that of our 20 ppm Stoddard Solvent standard. The concentration in the sample was approximately 10 ppm (mfg)• 0 0 Samples submitted: Date of Analysis: File ID: Analysis: Units: 4/22/96 5/2/96 04-063 HCID mg/Kg (ppm) Client: Global Environmental Project: AG Project#: Matrix: Soil Lab ID RESULTS Motor Surrogate Recovery Client ID Stoddard Gas Diesel Oil BFB O -TP 04-063-9 Quality Assurance B-3@10 <20 <20 <50 <100 120% 133% Method Blank <20 <20 <50 <100 91% 99% • Fi1e=c:\cp\may96c2\960502F4.04R Date printed = 05-02-1996 Time = 17:55:39 2.50 to 45.00 min. Low Y = - 0.10035 my High Y = 4.10035 my Span = 4.00000 my 4e_ }nC-9e 'i 1